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1 GPa Gas Pressure Regulators

The 1 GPa Gas Pressure Regulators supply continuously-loaded high-pressure cells with helium up to 1 GPa (10 kbar). Each system, built by SITEC, consists of a pneumatic-driven 2-head diaphragm compressor for pre-filling the system and the sample with helium up to 200 MPa, and a primary pump driving the pressure intensifier up to 1 GPa. The control loops and the different modes of control operation are performed on a Eurotherm Mini8 PLC. The graphical user interface is programmed with LabView on a panel PC with touch screen.

The pressure generation system is designed for controlled pressurisation and depressurisation. The pressure intensifier piston position is measured and indicated. If the piston has reached the upper end position, the automatic re-filling procedure is activated. In standard operation, NOMAD communicates via an Ethernet interface (Modbus TCP/IP) with the PLC. A list of the relevant PLC registers is provided below.

The compressors, pressure intensifier, valves, controller and related electronics are packed in a crate that is brought to the instruments. It also features two rollers of cables (230V and compressed air). The Florinert level in the tank is measured and indicated. On the GUI, the mode of operation can be changed to manual mode. In this mode, a simple pressure ramp up or down can be started. This makes it possible to test a pressure profile step by step.

PLC Registers (Eurotherm Mini8 Loop Controller)
Description Read Write Address

Actual value PT1 (intensifier outlet)

X

-

4228

Actual value PT2 (sample)

X

-

4229

Actual value PT3 (intensifier inlet)

X

-

4230

Actual pressure compressed air

X

-

4231

Piston position (intensifier)

X

-

4232

Filling level B1 (FC-770 Fluorinert level)

X

-

4233

Actual value PT4

X

-

4234

Emergency switch

X

-

4251

Output signal control valve compressed air

X

-

4252

Output signal control valve (intensifier pressure relief)

X

-

4253

Output signal control valve (sample pressure relief)

X

-

4254

Actual control phase

X

-

4962

Target set point (remote control)

X

X

4963

Intensifier ratio limit

X

-

4964

Maximum pressure

X

-

4965

Working set point

X

-

4966

Target set point (LabView)

X

-

4968

Remote control active

X

-

4969

Set point ramp rate

X

X

4970

Firmware version (Mini8)

X

-

4971

Offset PT1 (intensifier outlet)

X

-

4972

Offset PT2 (sample)

X

-

4973

Offset PT3 (intensifier inlet)

X

-

4974

Perform intensifier check

X

-

4975

Pressure increase disabled

X

-

4976

Ramp reached

X

-

4977

Timeout leak detection compressor (minutes)

X

X

4978

Leak detection enabled after programming start (hours)

X

X

4979

Reset "pressure increase disabled"

X

X

4980

Pressure alarm

X

-

5071