Injection Sticks

Injection stick for cryostats

Special sample sticks are available from a pool on request. Sufficient advance notice to sane(at)ill.fr is required for their reservation and preparation. These equipments are developed, repaired and modified by the Advanced Neutron Environment team.

These sample sticks are provided for carrying out gas sorption analysis experiments. The most recent ones feature two injection lines installed in a vacuum chamber with a Thermocoax heater. This avoids the cooling of the injected gas at the level of the nitrogen shield. A permanent flow can be maintained using the two independent capillaries. At present, the maximum injection pressure is 80 bar except for the stick 184ILHP49.

Sticks for gas injection available from the pool

Code	TemperatureRange (K)	MaximumPressure (bar)	Sample SpaceØ x height (mm)	Type, Comment
177ILGI49	2.6 - 320	3	Ø49	double-way, for PT cooler
184ILHP49	1.5 - 320	700	Ø49	single capillary with Thermocoax heater, for Orange crysotat
197ILGI49	1.5 - 320	200	Ø49	capillaries isolated in vacuum and attached to Thermocoax heater, for Orange cryostat
199ILGI70	1.5 - 320	200	Ø70	capillaries isolated in vacuum and attached to Thermocoax heater, for Orange cryostat
200ILGI49	2.6 - 320	3	Ø49	capilaries attached to Thermocoax heater, for PT cooler
205ILGI49	1.5 - 320	3	Ø49	single capillary and Quartz cell
223ILGI49	1.5 - 550	200	Ø49	ANSTO-HZB-ILL design
231ILGI70	1.5 - 550	200	Ø70	ANSTO-HZB-ILL design
242ILGI70	1.5 - 550	200	Ø70	ANSTO-HZB-ILL design
243ILGI49	1.5 - 550	200	Ø49	ANSTO-HZB-ILL design

Sticks for gas injection assigned to specific instruments

Instruments	Code	TemperatureRange (K)	MaximumPressure (bar)	Sample SpaceØ x height (mm)	Type, Comment
IN1 - Lagrange	213ILGI49	1.5 - 550	80	Ø49	ANSTO-HZB-ILL design
-	213ILGI70	1.5 - 320	80	Ø70	ANSTO-HZB-ILL design
IN8	237ILGI70	1.5 - 320	80	Ø70	ANSTO-HZB-ILL design
IN11	236ILGI49	1.5 - 320	3	Ø49	single capillary