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D11 Lowest momentum transfer & lowest background small-angle neutron scattering instrument

Characteristics

Guide hall n°1, vertical cold source V1, in-pile H1 insert, cold guide H15, channel H153 (deflector)
Monochromator
velocity selector
Eleanore/ Felicia (ASTRIUM standard selectors) variable, typically Δλ/λ = 9 % (FWHM)
incident wavelength variable, 0.46 ≤ λ [nm] ≤ 4
max. wavelength at max. detector dist. (39 m) λ = 2.2 nm
selector rotation normal to n-beam possibleminimum wavelength at rotation -7° -7° to + 7° λ = 0.32 nm
Collimation
17 guide sectionsstraight glass guides, m=1 (SwissNeutronics)elliptical focussing guides, m=1.5 (SwissNeutronics) side of square cross section14 straight guides 45 mm over 28.8 m 45 mm -> 47.65 mm from 5.6 to 4.1 m 47.65 mm -> 46.10 mm from 4.1 to 3.1 m 46.10 mm -> 38.0 mm from 3.1 to 1.6 m
guide-to-sample distances 1.6, 3.1, 4.1, 5.6, 6.7, 7.7, 10.2, 12.7, 15.2, 16.5, 17.8, 20.3, 22.8, 24.8, 26.9, 29.4, 31.9, 35.2 m (18 discrete distances)
4 variable-aperture slits (10B4C) at 34.63, 27.85, 6.74 and 1.65 m from sample
5 multiposition (8) aperture changer (10B4C) at 26.92, 20.38, 15.31, 10.28 and 5.70 m from sample
Attenuators
choice between 3 slitted cadmium sheets of different transmissions that can be combined to achieve 7 attenuation factors fa:fa=4.63 (att 1), fa=16.9 (att 2), fa=72.7 (att 3), fa=77.7 (att 1 + 2), fa=348 (att 1 + 3), fa=1165 (att 2 + 3), fa≈8200(att 1 + 2 + 3)
Sample area
flux at specimen at lowest resolution 1.2 · 10\(^{8}\)n·cm\(^{-2}\)·s\(^{-1}\) at λ = 0.6 nm at 55 MW (as measured on the detector)
typical sample size 7 × 10 mm\(^{2}\)
Detector
sample-to-detector distancesL continuously variable between 1.35 m and 38.9 m
typical momentum transfer range 3·10\(^{-3}\)≤ q [nm\(^{-1}\)] ≤ 6
detector type (since January 2021) \(^{3}\)He gas detector (256 1-m long, 8 mm outer diameter stacked tubes from Reuter-Stokes, installed in 3 panels, shaped as a cross of 1.5×1.5 m\(^{2}\): 192 horizontal tubes + 2 side panels of 32 tubes each. \(^{3}\)He at 10 bars. Stop-gas: Ar/CO2mix at 1.5 bars. Stainless steel 304 of 0.4 mm wall thickness. Operated at HV=1500 V.
efficiency 90, 95 and 99.5 % at λ = 0.45, 0.6 and 1 nm within the tubes. Due to the geometry of tubes assembly, 12 % of neutrons avoid the detection area.
area 2 m\(^{2}\)
pixel size 8 mm across (rectangular psf), 3 mm FWHM along tubes (Gaussian psf)
background 1.2 Hz on whole detector
detector deadtime 1.5 µs per tube (~1/10 event loss at 66 kHz per tube, at 225 kHz)
Content with side image d 11 375 x 375

Technical description

The polychromatic beam from the cold source is monochromated by a helical slot (ASTRIUM) velocity selector which selects neutrons of ±9 % about a mean wavelength determined by the rotation speed of the drum. The neutrons are then collimated by a series of moveable glass guides. Guide sections are inserted into or removed from the beam depending on the incident beam divergence required.

The sample zone, situated 35 m down-stream from the velocity selector, may be equipped with various sample environments such as an automatic temperature controlled sample changer, cryostat, magnet, shearing cell, Bohlin rheometer, dilution refrigerator, horizontal sample-changer under vacuum, etc.

Neutrons scattered from the sample are detected on a 1.5 x 1.5 m2 multi-PSD 3He detector mounted on a moveable trolley within the evacuated detector tube. The detector may be placed at any distance between 1.35 and 38.9 metres from the sample position, giving a typical momentum transfer range of 3 10-3 to 6 nm-1 that can be a bit extended for specific cases.

The D11 collimation system has been completely renovated between 2021 and 2025 (Endurance 2 renewal project).