operation mode is independent of gravityation, which makes it possible to follow the complex rotations of a 4-circle diffractometer. The technique used is similar to the one used on cryostats shipped on stra
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sample. The sample, usually a single crystal in a gas flow helium cryostat, is at the center of the eulerian cradle. The three axes ω,χ,ϕ of the Eulerian cradle are rotated until a given set of atomic planes ... D10 is set for a single crystal diffraction experiment in the 4-circle geometry. The polychromatic beam from the thermal neutron guide H24 ...
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monochromator, which selects a given wavelength. The monochromatic beam passes through slits to limit its size before reaching the sample. The sample, usually a single crystal in a gas flow helium cryostat ... The scattered beam, which may have a different wavelength from the incident beam, arrives on the analyser. To obtain the wavelength (or ...
Pertinence: 13%
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diffractometer. A similar technique is used for satellite cryostats. The movie shows the mounting of a new sample into the cryostat. the detector and the eulerian cradle are rotated to a position suitable ... 4-circle diffraction with a 3He dilution cryostat In the four-circle mode, the offset C-shaped Eulerian cradle can be equipped with a ...
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neutrons where there is a marked isotopic effect for helium (helium-4 is transparent, helium-3 is opaque to neutrons). Ref .: M. Enderle, S. Pujol, A. Hillenbach (Institut Laue-Langevin), A. Benoit (CRTBT CNRS) ... advanced dilution cryostat of D10 A neutron radiograph film recorded at the ILL in 2005 on NEUTROGRAPH shows the progressive dilution ...
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phase. The first transition is to a commensurate non-collinear antiferromagnetic structure, with a small spontaneous ferromagnetic component (Fig. 2); the second is to a helical structure where the phase ... the tetragonal c axis stays constant over a length L then changes abruptly over a short period ξ (Fig. 3). Close to T* the magnetic structure ...
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both in bond formation and cleavage. Could a similar analysis by structural correlation be applied to the reduction of ketonic carbonyl by hydride addition? A number of polycylic hydroxyketones, containing ... 04,8]decan-2-one (C12H16O2)These are viewed from similar directions nad o : denotes The structure of a cage compound at 30K The use of ...
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small-angle neutron scattering instrument D11 has been upgraded with a new primary guide and new collimation . D11 is the archetype of a long, pinhole geometry instrument for small angle neutron scattering ... matter systems, chemistry, biology, solid state physics and materials science. The instrument received a new 3 He multi-tube (Reuter-Stokes) ...
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Another typical experimental setup Here the sample area of D11 is equipped with a horizontal sample changer.
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The detector tank D11 with its new colors after its upgrade with a larger and faster detector, new collimating guides, etc. This photo makes it possible to assess the length of the detector tank.
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