Trouble Shooting Guide
Trouble Shooting Guide
Anomaly | Possible Cause | Remedy |
---|---|---|
Cryostat body wet after liquid nitrogen filling. | Poor vacuum. Vacuum valve not fully closed. Vacuum leak. | Pump the vacuum. Close the vacuum valve. Pump continuously and inform us. |
Cryostat will not receive liquid helium. | No liquid nitrogen. Helium leak. Contact between shields. | Fill liquid nitrogen bath. Pump continuously and inform us. Return the cryostat to our lab. |
Sample cools badly and high flow necessary to stabilise T < 50K. | Contact between shields. | Return the cryostat to our lab. |
Cold valve blocked. | Cryostat badly flushed. | Reheat to 300K and inform us. |
Temperature rises rapidly after closing cold valve. | Sample still warm. | Wait for thermal equilibrium of sample and exchanger. |
Cooling difficult with temperature oscillations. | Wrong PID settings and/or too much exchange gas. | Check the PID settings, set T=10K and pump via exchange gas valve to <1mbar. |
Fluctuations at low temperature (T<4.2 K), unstable cold valve pressure, cold valve pressure rise when heating | Liquid helium in the annular enclosure (tail). | Close cold valve, set T=10K and wait until the pressure drops to < 2mbar. |
Temperature rises for no apparent reason. | Lack of liquid nitrogen and/or liquid helium. | Verify the liquid helium and liquid nitrogen levels, refill. |
Sample stick stuck in cryostat. | Air leak into sample well. | Go to 150K by step of 20K with the clamp slightly unscrewed. DO NOT FORCE AND DO NOT STAY ABOVE THE STICK. |