Large dynamic range small-angle diffractometer D22

Small-angle scattering is a technique that measures the deviation to small angles (much less than one degree to several degrees) of an X-ray or neutron beam due to structures of small size in the sample. “Small” means dimensions of a few tenths to about 100 nanometres, such as clusters in alloys, polymers, or biological macromolecules.

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Fast Detector

Detector

In order to provide the necessary accuracy of the anode centring in the tube, each one of the 128 PSD has to be mounted on the mechanical support with 2 precise flanges.

All PSD, including spares, have been radiographied by X-rays. These radiographies will help to set up a relationship between possible failures and mechanical defects: for example, several PSDs show a misalignment between the spring guide and the tube wall up to 0.5 mm; this misalignment creates the potential danger of anode breaking when the High Voltage is ON.

The fragility of the PSD is now considered as the major remaining risk in the project. Moving the detector when the High voltage is ON would probably destroy some PSDs. A circuit is being developed to discharge the 2 decoupling capacitors (68 nF) of each PSD before any displacment of the detector.

Instrument

D22 millenium

Sort

position sensitive cylindrical counter

Manufacturer

REUTER STOKES

Number of detectors

128

Gas

3He / Ar / CO2

Pressure

15 bars

tube material

stainless steel 304L, 0.4 mm thick

Electronic

charge division method

Coding

1D

Dimension

1000x8 mm²

Resolution

6 mm FWHM

Hight voltage value

1550 V

To top

To top

Position on the detector

ILL's ref (select to see the P.H. spectrum)

RS ref (select to see the X-Ray radiography)

Resistance's value (kOhms)

Comments

 

8.017

 


 

8.036

 


 

8.046

 


 

7.935

 


 

8.019

 


 

7.96

 


 

8.035

 


 

7.941

 


 

7.959

 


 

8.005

 


 

7.949

 


 

12

8.37

 


 

13

7.988

 


 

14

7.977

HS

 

15

7.939

 


 

16

7.956

 


 

17

8.007

HS

 

8.111

 


 

7.966

 


 

7.94

 


 

7.99

 


 

8.031

 


 

7.982

 


 

7.936

 


 

7.94

 


 

8.011

 


 

7.96

 


 

7.841

 


 

8.025

 


 

7.969

 


 

7.97

 


 

7.987

 


 

7.988

 


 

7.949

 


 

8.024

 


 

7.975

 


 

8

 


 

7.985

 


 

8

 


 

7.997

 


 

7.996

 


 

7.998

 


 

8.007

 


 

7.98

 


 

7.966

 


 

7.955

 


 

8.006

 


 

8.066

 


 

7.963

 


 

7.955

 


 

7.958

 


 

7.977

 


 

8.015

 


 

7.956

 


 

7.942

 


 

7.953

 


 

7.971

 


 

7.968

 


 

8.019

 


 

7.945

 


 

7.985

 


 

7.982

 


 

7.997

 


 

7.994

 


 

7.981

 


 

7.968

 


 

8.089

 


 

7.985

 


 

7.908

 


 

8.094

 


 

7.972

 


 

7.978

 


 

8.006

 


 

7.975

 


 

7.944

 


 

8.009

 


 

7.987

 


 

7.944

 


 

7.941

 


 

7.928

 


 

8.013

 


 

7.971

 


 

7.998

 


 

7.984

 


 

7.997

 


 

8.063

 


 

7.935

 


 

8.013

 


 

7.979

 


 

7.97

 


 

7.938

 


 

8.05

 


 

8.003

 


 

7.987

 


 

8.075

 


 

7.942

 


 

7.968

 


 

8.109

 


 

7.97

 


 

7.942

 


 

7.94

 


 

7.95

 


 

8.047

 


 

7.973

 


 

8.008

 


 

7.998

 


 

8.008

 


 

7.98

 


 

7.965

 


 

7.991

 


 

7.967

 


 

8.003

 


 

8.117

 


 

7.991

 


 

7.993

 


 

7.983

 


 

7.964

 


 

8.028

 


 

8.044

 


 

8.068

 


 

8.01

 


 

7.995

 


 

8.009

 


 

7.945

 


 

7.946

 


 

7.997

 


 

8.043

 


 

7.999

 


 

7.929

 


 

7.988

 


 

7.96

 


 

7.944

 


 

7.969

 


 

7.951

 


 

7.982

 


 

7.944

 


 

137

8.029

 


 

8.039

 


 

8.086

 


 

8.021

 


 

141

7.96

 


 

7.95

 


 

8.012

 


 

7.984