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Small-angle scattering is a technique that measures the deviation to small angles (much less than one degree to several degrees) of an X-ray or neutron beam due to structures of small size in the sample. “Small” means dimensions of a few tenths to about 100 nanometres, such as clusters in alloys, polymers, or biological macromolecules.

D22 emergency proceduresKeep cool, baby!
Information about D22 can be found on the D22 yellow page in ILL's WWW server. See also the D22 documentation and the D22 Short Manual. Contents of this manual1. Partially missing detector imageIn particular after a restart of MAD, parts of the detector (vertical stripes) may not be counting. In this case, go to the detector acquisition cabin, open the door of the electronics cabinet (after pushing on the buton below the black handle) and push the four reset buttons of the crates where the 256 brown signal cable arrive. The reset buttons (marked RST) are found on crates that are each positioned in the middle of four crates with lemo connectors. 2. Power failure on supervision PC
Choose "Gestionnaire de fichiers" In there, choose "InTouch", "View" It may be necessary to initialize also the cooling system and the vacuum pumps (see below). 3. Initialization of selector and detector cooling unit
4. Selector restartThe selector normally runs under MAD; if it stops due to an emergency event shown by the red EMERGENCY field in the selector program window on the supervision PC, you should first check whether the emergency is real or a fault of the security system. In the first case, have the fault repaired and reset D22's process controller (ACQUIT DEFAUT button on the central cabinet). In the latter case, just reset. For restarting the selector after an emergency eveny, it is normally sufficient to push the RESTART button on the selector power supply. This is situated in the lower part of the rightmost cabinet of D22's process controller. If after 5 attempts to restart there has been no success, another RESET is necessary. If the selector program does not react to any attempt to modify the speed, check whether the selector power supply is on COMPUTER CONTROL. If this is the case, think of restarting the selector program (see below). 5. Selector supervision program restartThe selector supervision program ("Anatole") can be found on the supervision PC in the "Gestionnaire de programmes" in the InTouch directory. The password is "ILL". Anatole starts in local mode. The program requires a start value: Click on the CONTROL button and enter an allowed speed value. When this value is reached and stable, you may switch to VAX control by choosing the corresponding menu item ("controle_vax") of the selector program window. If the values imposed by the instrument computer are not read by the selector program although it is in VAX mode, it may also be necessary to restart the communication program MODBUS. Check whether the communication is active: On top of the control PC (under the table), there is a box (westermo) where the RD and TD indicators should blink. If this is not the case, quit MODBUS and start it again from the "Gestionnaire de programmes". (Quit a window program by clicking its icon and choosing "fermeture" from the menu. It might be necessary to shrink other windows to see the application's icon). 6. Initialization of vacuum pumps
Vax control is switched on again automatically by issuing a MAD command addressing the PC, e.g. SEL. 7. Collimation time-outEspecially after a shut-down, the collimation change may fail because the positioning pistons have got stuck. If the collimation times out before indicating a correct position, another movement of the collimation is not possible (Message "Collimation is already running"). In this case, wait for the collimation movement to stop,
Then type COLL on the MAD terminal and check the current collimation value. After that, a new COLL command should work. It might be necessary to push the "ACQUIT DEFAUT" button on the control cabinet in the guide hall. In manual mode, the "START" button (InTouch collimation screen) can be used for setting the collimation. 8. Power failure on process control cabinetIn case of a power failure of the process control cabinet, rearm the main switch "ARMOIRE CONTROLE COMMANDE", bottom right in the electric cabinet "COFFRET CAR D22" in the hall ILL22, next to the door of the D22 cabin, on the right hand side seen from the hall. If such a power failure happens, also the pumping and cooling systems and the selector stop (see above). 9. Acquisition errorIn the case of an error "Cannot initialize acquisition (check VME)", check whether the red status light of the acquisition card (ILL-TOF), slot 16 in top VME rack, is "half lit". If it isn't
10. Low fluxMain reasons for a lower flux than expected are
11. Restarting MADIf MAD does not respond to commands, you need to restart all MAD processes. First, all remaining MAD processes need to be killed (use an Xterm window on the acquisition workstation d22a other than the one running MAD): /users/mad/MADKILL/madkill [cr] Second, you need to restart MAD (in the window where it was running previously or a new one): type mad [cr] (as /users/d22) 12. Rebooting the acquisition workstation d22 (Dec alpha)If none of the windows on the acquisition workstation respond to commands, you may try to switch sessions. Normally you are using the "MAD" session. Try to switch to another session by clicking on "TWO" etc. in the toolbar at the bottom of the workstation screen and go back to the "MAD" session. If nothing helps, reboot the acquisition workstation:
13. Problems with detector high voltage(Version 2, March 2005, contributed by Patrick van Esch) 13.1. Description of the systemThe system consists of two units: one is the High voltage (HV) controller and the other is the HV filter. The HV controller (pdf) is in the grey metal box next to the HV supply in the electronics bay in the cabin. The HV filter is mounted inside the cone behind the detector, in the grey metal box on the left side (the upper box ; the lower box is the low voltage distribution box). Both units are interconnected with 3 lemo cables (of which 2 are "double cables", with two successive cable numbers), named "charge rapide", "decharge" and "mesure". The HV cable number 1 goes directly from the HV power supply onto the HV filter. HV cable 2 is a spare cable. 13.1.1. The HV filterThe HV filter box applies the HV to the detector and can also discharge the detector. There are two HV relays that do this. It also measures the HV on the detector through a resistive divider (divides by 1000). The symbolic scheme is the following: +----(relay 1)----+ Relay 1 is a passively OPEN relay, which closes (makes contact) when we put a voltage on "charge rapide". Relay 2 is a passively CLOSED relay, which shortens the HV output to ground. When we put a voltage on "decharge", the relay opens (breaks contact with ground) and hence permits a voltage to be present on the detector. This has been choosen for security: if ever the relay cable is cut or disconnected, the detector will discharge (most secure situation).
If relay 2 is not activated (we 'discharge' the detector) and relay 1 is activated (currently this is always the case) then we will also shorten the HV supply ; we want to avoid this situation (as it is thought to be a cause of a sticking relay 2 due to the sudden discharge of the capacity of the HV cable through relay 2). When the detector is discharged, relay 1 will be open. THIS HAS THE EFFECT THAT 1515V WILL REMAIN VISIBLE ON THE HV SUPPLY EVEN IF THE DETECTOR IS DISCHARGED. There is no visual indication anymore of the voltage on the detector. The voltage divider divides the voltage measured on the HV out by 1000, and this voltage is present on "mesure". The normal working situation is the following: relay 1 is open (not powered), and relay 2 is open (is powered). The detector is then under HV, through the filter. 13.1.2. The HV controllerThe HV controller (pdf) is based upon an industrial process controller. It is powered through two 12 V adapters in the power outlet on the back of the electronics bay for functioning. It has ADC inputs and it has relays as outputs. The configuration is the following: Input 5: HV "mesure" signal (on an ADC input) MODIFICATION JAN/2005: There are now two lemo cables in parallel leading to relay 1 and relay 2; they are connected together with a lemo-T on both sides (on the controller in thebay, and inside the cone on the detector side). So where we read "the discharge cable" we mean the two cables together of course. This has been done to secure better the link between the controller and the relays, and to reduce the voltage drop through the cables.
The controller has two independent functions: HV control and movement security.
There is however a way to find out if the detector is discharged or not, and that is BY LOOKING AT THE CURRENT OF THE HV SUPPLY. (Turn the round knob to "I" instead of "V"). 13.2. Emergency proceduresTo check whether the detector is at 0 V, go to the HV supply (which should always indicate the nominal voltage, 1515V), and turn the knob of the readout to "I". If the reading is something like 0.02, then the detector is normally under tension (the small current of 15 microamps is the result of the voltage divider of 100M). If the reading is something like 0.84, then the detector is discharged and the current is the one flowing through the 1M8 RC filter. 13.2.1. Problem: the HV supply indicates that the detector is at 0 V without a reasonCheck whether the supply is in "current limit mode". If not, there is a problem with the HV supply (or the voltage is set to 0 V; set it to 1515 V). Check that the lemo connectors of the double cable with "decharge" (and also the blue scotch on it) is well connected to the unit. Unplug it and plug it in again. If that doesn't help, plug that double cable in the free 6 V outlet in the grey box next to the 12V supply (so we force the discharge relay to open). This should work. IF IT DOESN'T, go to topic "Discharge relay is stuck". If this allows the HV on the detector to go up again (current falls from 0.84 to 0.02), check whether the controller is working (see topic "The controller is not working"). If the controller is working, the relay is not stuck but it doesn't work when you put it onto the control unit, check whether you are allowed to move the detector when it is discharged (0.84 current). If that's the case, you can go to topic "Partially manual mode". If this is not the case, go to topic "Live dangerously". 13.2.2. Problem: the high voltage is 0 on the detector, but I'm not allowed to move the detector.Check whether the red and green leds next to the motor controllers (on top of the led box) in the control room are lit when you ask to move. If they are lit, it is a problem with the SCI, not with the detector. Unplug and replug the cable "mesure" on the control unit. Measure de voltage on the that cable (by finding a lemo base and a multimeter). You should read the voltage on the detector, divided by 1000. So if you find about 1.5 V, then the detector is NOT at 0 V; if you find a very low voltage, then this should normally work; in this case, try to measure the resistance of the wire: you should find 100 kOhm (if not, there's something wrong with with this cable). Warning: only measure that resistance when all HV has been removed! Go to topic "Live dangerously". Note: it is normal that you have to wait for 7 seconds before you are allowed to move the detector. 13.2.3. Problem: I give a movement command, but the detector stays at 1515 V.Unplug and plug in the LEMO cables from the SCI on the controller (lemo 1 and lemo 2). Check whether the controller is working (see "the controller is not working"). You might ask an SCI responsible (e.g. Jean Vidal) to check whether his signals arrive at the controller or not. Check whether the 6 V supply lemo cable is well connected to the grey box next to the 12 V supply. Check whether the +6 V supply of the amplifiers is up and running (has 6.06 V or so on its display). If you do not succeed, go to topic "partially manual mode". 13.2.4. The controller is not workingTake the box and look on the LCD display. In the upper left corner, there should be a small "wheel" turning. If not, try to switch it on again. If the display is blank, check whether the two 12 V adapters on the back of the rack (go around, open the back door) are plugged in. It might help to unplug them, wait a minute, and plug them in again to restart the controller. If you do not succeed, go to topic LIVE DANGEROUSLY. 13.2.5. The discharge relay is stuckIf the discharge relay is stuck even after plugging it into the 6 V supply, try to find a power supply with banana connectors, and take the small tool (a piece of pcb with some lemo bases on it with a black and a red banana cable). Take the "discharge" cable (with the blue label) and plug it into the tool, connected to a supply. Put 7 or 8 V on it: hopefully now the relay gets released. Test whether it works now on 6 V using the 6 V supply. If it is ok, we can go back to normal automatic mode. If not, go to topic "partially manual mode". 13.2.6. Partially manual modeThere are different levels, according to the problem at hand. The simplest case is that we leave the "discharge" cable plugged into the control unit, but we switch off the HV supply and wait a minute or so before giving movement commands. We can also plug the "discharge" cable into the 6 V supply. Finally, we might need to plug it into the small tool (from topic 13.2.5) and keep it at 7 or 8 V. Check whether you can move the detector after waiting for a minute after switching off the HV. If not, go to topic 13.2.2. In this mode, the controller still functions as a security device, so security is still guaranteed. 13.2.7. Live dangerouslyThis mode of operation is highly discouraged, because one single error can easily kill a 2,000,000.00 Francs detector. You are highly discouraged to do this. Is it really worth to risk to sacrifice the whole detector just for a few hours/days of beam? OK, you still want to do so ? Find a Lemo T-piece and connect lemo 1 and lemo 2 from the SCI together. IT IS YOUR PERSONAL RESPONSABILITY TO MAKE SURE THAT THE BIG PLUG IS NEVER ON THE CABLE WHEN THE HV UNIT IS POWERED. |