|
|
|
The large structures diffractometer D19 is the monochromatic thermal neutron single crystal diffractometer of choice for determination of crystal structures with unit cells in the range of 102 to 106 Ǻ3.

PublicationsNanofibrillar Structure and Molecular Mobility in Spider Dragline Silk, Sapede, D., Seydel, T., Forsyth, V.T., Koza, M.M., Schweins, R., Vollrath, F., Riekel, C., Macromolecules (in press). Combined X-ray and Neutron Fbre Diffraction Studies of Biological and Synthetic Polymers, I.M. Parrot, V. Urban, K.H. Gardner, V.T. Forsyth, Nuc. Inst. Meth. B (in press). New insights into the structure of poly(p-phenylene terephthalamide) from neutron fiber diffraction studies, Gardner, K.H., English, A.D., Forsyth, V.T., Macromolecules 37, 9654-9656 (2004). Water-DNA interactions by x-ray and neutron fibre diffraction, Fuller, W., Forsyth, V.T. and A.Mahendrasingam, Phil. Trans. Roy. Soc. 359, 1448, pp 1237-1248 (2004). Comparative Neutron and X-ray study of [PPN][HIr4(CO)9( - Ph2PCH2PPh2)], Detti, S., Forsyth, V.T., Roulet, R., Ros, R., Tassan, A., Schenk, K. J., Zeitschrift für Kristallographie 219, 47-53 (2004). Crystal Structure and Hydrogen Bonding System in Cellulose Iα from Synchrotron X-ray and Neutron Fiber Diffraction, Nishiyama, Y., Sugiyama, J., Chanzy, H., Langan, P., J. Am. Chem. Soc. 125, 14300-14306 (2003). (See also Cellulose stacks up, Jarvis, M., Nature 426, 611-612 (2003) for News and Views report on this work) Intramolecular vs Intermolecular Hydrogen Bonding of Coordinated Acetate to Organic Acids: A Neutron, X-ray and Database Study, Vives,G., Mason, S.A., Prince, P.D., Junk, P. Steed, J.W., Crystal Growth & Design 3, 699 (2003). Anisotropic Thermal Expansion in 18-crown-6 · 2 H2O · 2 HNO3, M. Calleja, S. A. Mason, P. D. Prince, J. W. Steed, C. Wilkinson, New J. Chem. 27, 28-31 (2003). Preparation of Tunicin cellulose Ib samples for x-ray and neutron diffraction, Nishiyama, Y., Langan, P., Chanzy, H., Fib. Diff. Rev. 12, 75-78 (2002). Structural studies of biological & synthetic polymers using x-ray and neutron diffraction, Forsyth, V.T. , Gardner, K., Parrot, I. and Langan, P. Polymer Preprints 43, 1, 173-175 (2002). On the reliability of C-H…O in Crystal Engineering: Synthesis and Structure of Two Hydrogen Bonded Phosphonium Bis(aryloxide) Salts, Broder CK, Davidson MG, Forsyth VT, Howard JAK, Lamb S, Mason SA, Cryst. Growth Des., 163-169, 2, (2002). Crystal Structure and Hydrogen Bonding System in Cellulose Ib from Synchrotron X-ray and Neutron Fiber Diffraction, Nishiyama, Y., Langan, P., Chanzy, H., J. Am. Chem. Soc. 124, 9074-9082 (2002). Synchrotron x-ray and neutron fiber diffraction studies of cellulose polymorphs, Nishiyama, Y., Chanzy, H., Wada, M., Sugiyama, J., Mazeau, K, Forsyth, V.T., Riekel, C., Mueller, M., Rasmussen, B., Langan, P. (2001) , Advances in X-ray analysis, 44, pp 102-104 A fast new diffractometer for chemical crystallography, small proteins and fibre diffraction, Forsyth, V.T. , Mason, S. A., Howard, J. A. K., Davidson, M. G., Fuller, W. and Myles, D. A. A. Neutron News, 12, 4, pp 10-15 (2001). Single Crystal Neutron and X-ray Diffraction Studies of (H7O3)[AuCl4]·15-crown-5, M. Calleja, S. A. Mason, P. D. Prince, J. W. Steed and C. Wilkinson, New J. Chem. 25, 1475–1478 (2001). Neutron Diffraction Study of a Phenol-Nitroxide Radical Adduct: A Structural Model for Hydrogen Atom Abstraction by Peroxyl Radicals from Vitamin E and related Phenolic Antioxidants, Ahrens B, Davidson MG, Forsyth VT, Mahon MF, Johnson AL, Mason SA, Price RD, Raithby PR, J. Am. Chem. Soc., 9164-9165, 123, (2001). D19: A fast new diffractometer for chemical crystallography, small proteins and fibre diffraction, Mason, S. A., Forsyth, V.T. , Howard, J. A. K., Davidson, M. G., Fuller, W. and Myles, D. A., in J. DIANOUX (Ed) Opportunities for Neutron Scattering in the 3rd Millennium (Institut Laue Langevin publication) 332-334 (2001). High resolution neutron fibre diffraction data on hydrogenated and deuterated cellulose, Y. Nishiyama, T. Okano, P. Langan, H. Chanzy, Int. J. Biol. Macr. 26 (4), 279-283 (1999). A revised structure and hydrogen bonding system in cellulose II from a neutron fibre diffraction analysis, P. Langan, Y. Nishiyama and H. Chanzy, J. Am. Chem Soc. 121 (43) 9940-9946 (1999). Neutron Laue diffraction studies of coenzyme cob(II)alamin, P. Langan, M. Lehmann, C. Wilkinson, G. Jogl and C. Kratky, Acta Cryst. D55, 51-59 (1999). Instrument D19 at the Institut Laue-Langevin: A High Resolution Diffractometer for Single Crystal and Fibre Diffraction Studies, V.T. Forsyth, M.W. Shotton, H. Ye, C. Boote, P. Langan, L.H. Pope, R.C. Denny, Fibre Diffraction Review 7, 17-24 (1998). New developments in instrumentation for fibre diffraction experiments, M. W. Shotton, L.H. Pope, V.T. Forsyth, R.C. Denny, J. Archer, P. Langan, H. Ye, C. Boote, J. Appl. Cryst. 31 (5), 758-766 (1998). Neutron diffraction study of [K(18-crown-6)][(PPh3)2ReH6Cr(CO)3], a bimetallic donor-acceptor complex, DRABNIS M.H., BAU R., MASON S.A., FREEMAN J.W., ERNST R.D., European Journal of Inorganic Chemistry199, 851-854 (1998). A high-angle neutron fibre diffraction study of the hydration of B-DNA, M. W. Shotton, L. H. Pope, V. T. Forsyth, P. Langan, H. Grimm, A. Rupprecht, R. C. Denny and W. Fuller, Physica B 241-243, 1166-1168 (1998). Refinement of the incommensurate structure of high quality Bi-2212 single crystals from a neutron diffraction study, MILES P.A., KENNEDY S.J., MCINTYRE G.J., GU G.D., RUSSELL G.J., KOSHIZUKA N., Physica C 294, 275-288 (1998) Ordered water around deuterated A-DNA by neutron fibre diffraction, L.H. Pope, M.W. Shotton, V.T. Forsyth, P. Langan, R.C. Denny, U. Giesen, M.T. Dauvergne and W. Fuller, Physica B 241-243, 1156-1158 (1998). Syntheses of the uranium complexes [U{N(SiMe3)2}2{N(SiMe3)(SiMe2CH2B(C6F5)3)}] and [U{C(Ph)(NSiMe3)2}2{mu3-BH4}2]. Determination of hydrogen positions by single-crystal x-ray and neutron diffraction, MUELLER M., WILLIAMS V.C., DOERRER L.H., LEECH M.A., MASON S.A., GREEN M.L.H., PROUT K., Inorganic Chemistry 37, 1315-1323 (1998). A high-angle neutron fibre diffraction study of the hydration of deuterated A-DNA, Mark W. Shotton, Lisa H. Pope, Trevor Forsyth, Paul Langan, Richard C. Denny, Ursula Giesen, Marie-Therese Dauvergne, Watson Fuller, Biophysical Chemistry 69 (1), 85-96 (1997). [ISSN 0301-4662]. Crystal engineering and correspondence between molecular and crystal structures. Are 2- and 3-aminophenols anomalous?, ALLEN F.H., HOY V.J., HOWARD J.A.K., THALLADI V.R., DESIRAJU, G.R., WILSON C.C., MCINTYRE G.J., Journal of the American Chemical Society 119, 3477-3480 (1997). Neutron diffraction study of aromatic hydrogen bonds: 5-ethynyl-5H-dibenzo[a,d]cyclohepten-5-ol at 20K, STEINER T., MASON S.A., TAMM M., Acta Crystallographica B 53, 843-848 (1997). The distribution of water in highly ordered fibres of hyaluronic acid, DERIU A., CAVATORTA F., DE MICHELI T., RUPPRECHT A., LANGAN P., Physica B 234-236, 215 (1997). Neutron diffraction analysis of H2Os6(CO)18, R. Bau, S.A. Mason, L. Li, W.T. Wong, J. Am. Chem. Soc. 119 , 11992 (1997). Disorder of decagonal AlCoNi, AlNiFe and AlCoCu phases studied by diffuse x-ray and neutron diffraction, FREY F., HRADIL K., GRUSHKO B., MCINTYRE G.J. in Quasicrystals (World Scientific Publishers) (1997). Diffuse features in neutron diffraction studies of high quality Bi-2212 single crystals, MILES P.A., KENNEDY S.J., MCINTYRE G.J., GU G.D., RUSSELL G.J., KOSHIZUKA N., Physica C280, 66-70 (1997). Neutron fibre diffraction: Recent advances at the ILL, P. Langan, Physica B 234-236, 213 (1997). Neutron Laue diffraction study of concanavalin A: the proton of ASP28, HABASH J., RAFTERY J., WEISGERBER S., CASSETTA A., LEHMANN M.S., HOGHOJ P., WILKINSON C., CAMPBELL J.W., HELLIWELL J.R., Journal of the Chemical Society Faraday 93, 4313-4317 (1997). Tests of the LADI image-plate detector on D19, Langan P., Myles D.A.A., Lehmann M.S., Wilkinson C., Mason S.A., Institut Laue-Langevin internal report ILL97LA01T (1997). Single crystal diffractometry with area detectors : application to twinned crystals, incommensurate structures and quasi-crystals, MCINTYRE G.J., Structure and Properties of Crystalline Materials (Frank Laboratory of Neutron Physics Joint Institute for Nuclear Research, Dubna, Russia) Time-of-flight neutron Laue fibre diffraction studies of perdeuterated DNA, V.T.Forsyth, P. Langan, M. A. Whalley, A. Mahendrasingam, C.C. Wilson, U. Giesen, M.-Th. Dauvergne, S.A. Mason, W. Fuller, in Neutrons in Biology (Eds B. P. Schoenborn and R. Knott), Chapter 30 (pp 359-367) (Plenum, 1996). Structural investigations of the ionic conductivity in zirconia single crystals by neutron diffraction at high temperatures and simultaneously applied electric field, KAHLERT H., FREY F., BOYSEN H., PROFFEN T., MASON S.A., WEPPNER W., Ionics 2, 88-96 (1996). DNA hydration studied by neutron fibre diffraction, W. Fuller, V.T. Forsyth, A. Mahendrasingam, P. Langan, W.J. Pigram, S.A. Mason, C.C. Wilson, in Neutrons in Biology (Eds B. P. Schoenborn and R. Knott), Chapter 29 (pp 345-358) (Plenum, 1996). A neutron image plate quasi-Laue diffractometer for protein crystallography, CIPRIANI F., CASTAGNA J.C., WILKINSON C., LEHMANN M.S., BUELDT G., in Neutrons in Biology (Eds B. P. Schoenborn and R. Knott), 423-431 (Plenum, 1996). Collecting and processing neutron fibre diffraction data from a single-crystal diffractometer, P. Langan, R.C. Denny, A. Mahendrasingam, S. Mason, A. Jaber, J. Appl. Cryst. 29, 383 (1996). Attenuation corrections for x-ray and neutron fibre diffraction studies, P. Langan, V.T. Forsyth, A. Mahendrasingam, J. Appl. Cryst. 28, 49 (1995). Structural studies of biological and industrial fibres using synchrotron radiation sources and neutron beams, W. Fuller, A. Mahendrasingam, V.T. Forsyth, Acta Chim. Slov. 42 (2), 257 (1995). Neutron fibre diffraction studies of DNA hydration, P. Langan, V.T. Forsyth, A. Mahendrasingam, U. Giesen, M.-Th. Dauvergne, S.A. Mason, C.C. Wilson, W. Fuller, Physica B 213/214, 783 (1995). mcFibre; Software for analysing data collected on D19 in fibre precession geometry, Shotton M., Langan P., Institut Laue Langevin internal report ILL95SH12T (1995). High-resolution neutron study of vitamin B12 coenzyme at 15K: solvent structure, Bouquiere J.P., Finney J.L., Savage H.F.J., Acta Crystallographica B 50, 566-578 (1994). Thermal evolution of the crystal structure of the rhombohedral Bi0.75Sr0.25O1.375 phase: a single crystal neutron diffraction study, MERCURIO D., CHAMPARNAUD-MESJARD J.C., FRIT B., CONFLANT P., BOIVIN J.C., VOGT T., Journal of Solid State Chemistry112, 1-8 (1994). Lengthening of the covalent O-H bond in O-H...O hydrogen bonds re-examined from low-temperature neutron diffraction data of organic compounds, STEINER T., SAENGER W., Acta Crystallographica B50, 348-357 (1994). Neutron diffraction structure of alpha-cyclodextrin cyclopentanone hydrate at 20 K: Host-guest interactive disorder, LEBAS G., MASON S.A., Acta Crystallographica B50, 717-724 (1994). High-resolution neutron study of vitamin B12 coenzyme at 15 K : Structure analysis and comparison with the structure at 279 K, BOUQUIERE J.P., FINNEY J.L., LEHMANN M.S., LINDLEY P.F., SAVAGE H.F.J., Acta CrystallographicaB49, 79-89 (1993). Fibre Diffraction, V.T. Forsyth, Chapter XI, HERCULES Volume I: Neutron and synchrotron radiation for condensed matter studies (Eds Baruchel, Hodeaue, Lehmann, Regnard, Sclenker) (1993). Single-crystal diffractometry with monochromatic x-rays and neutrons , MCINTYRE G.J., HERCULES Volume I: Neutron and synchrotron radiation for condensed matter studies (Eds Baruchel, Hodeaue, Lehmann, Regnard, Sclenker) (1993). Interaction of the tetramethylammonium ion with the lysozyme molecule, studied using neutron diffraction, BOUQUIERE J.P., FINNEY J.L., LEHMANN M.S., Journal of the Chemical Society Faraday Transactions 89, 2701-2705 (1993). Distribution of observed C-H bond lengths in neutron crystal structures and temperature dependence of the mean values, Steiner T., Saenger W., Acta Crystallographica A49, 379-384 (1993). Complementary x-ray and neutron fibre diffraction studies of the distribution of water and cations around the A-DNA double helix, P. Langan, V.T. Forsyth, A. Mahendrasingam, D. Alexeev, S.A. Mason, W. Fuller, Proc. Ital. Phys. Soc. 43, 235 (1993). Role of C-H...O hydrogen bonds in the coordination of water molecules. Analysis of neutron diffraction data, Steiner T., Saenger W., Journal of the American Chemical Society 115, 4540-4547 (1993). The location of ions and water around the D conformation of DNA, V.T. Forsyth, P. Langan, A. Mahendrasingam, S.A. Mason, W. Fuller, Proc. Ital. Phys. Soc. 43, 231 (1993). The experimental electron density in monoclinic cobalt sulfate hexahydrate, CoSO4.6D2O, at 25K, Kellersohn T., Delaplane R.G., Olovsson I., Mcintyre G.J., Acta Crystallographica B49, 179-192 (1993). Covalent bond lengthening in hydroxyl groups involved in three-center and in cooperative hydrogen bonds. Analysis of low-temperature neutron diffraction data, Steiner T., Saenger W., Journal of the American Chemical Society 114, 7123-7126 (1992). A neutron diffration study of the distribution of water in the A form of the DNA double helix, P. Langan, V.T. Forsyth, A. Mahendrasingam, D. Alexeev, W. Fuller, S.A. Mason, Physica B180/181, 759-761 (1992). Single-crystal neutron diffraction study of metamict zircon up to 2000 K, Mursic Z., Vogt T., Boysen H., Frey F., Journal of Applied Crystallography 25, 519-523 (1992). Geometric analysis of non-ionic O-H...O hydrogen bonds and non-bonding arrangements in neutron diffraction studies of carbohydrates, Steiner T., Saenger W., Acta Crystallographica B48, 819-827 (1992). High-angle neutron fibre diffraction studies of the distribution of water around the D form of DNA, V.T. Forsyth, A. Mahendrasingam, P. Langan, Y. Al-Hayalee, D. Alexeev, W.J. Pigram, W. Fuller, S.A. Mason, Physica B 180/181, 737-739 (1992). Structural instabilities of the trigonally coordinated water molecules in Ba(IO3)2.H2O and Pb(CIO3)2.H2O studied by X-ray and neutron diffraction at 25 and 295 K, Kellerssohn T., Lutz H.D., Vogt T., Delaplane R.G., Olovsson I., Acta Crystallographica B48, 166-172 (1992). Geometry of C-H...O hydrogen bonds in carbohydrate crystal structures. Analysis of neutron diffraction data, Steiner T., Saenger W., Journal of the American Chemical Society114, 10146-10154 (1992). A high-angle neutron fibre diffraction study of the hydration of the A conformation of the DNA double helix, P. Langan, V.T. Forsyth, A. Mahendrasingam, W. J. Pigram, S.A. Mason, W. Fuller, J. Biomol. Str. Dyn. 10 (3), 489 (1992). Low-temperature neutron diffraction study of [ReH5(PPhiPr2)2(SiHPh2)2] and low-temperature X-ray diffraction study of [ReH5(PCyp3)2(SiH2Ph)2], Howard J.A.K., Keller P.A., Vogt T., Taylor A.L., Dix N.D., Spencer J.L., Acta Crystallographica B48, 438-444 (1992). Neutron diffraction studies of the structure of PEEK, A.Mahendrasingam,Y.Al-Hayalee, V.T. Forsyth, P. Langan, W. Fuller, R.J. Oldman, D.J. Blundell, S.A. Mason, Physica B180/181, 528-530 (1992). The structure and magnetic characteristics of a holmium-1, 2, 3 superconductor with tetragonal symmetry, Arabi H., Ciomartan D.A., Clamp M.E., Mitchell P.W., Ross J.W., Sandiford D.J., Mills O.S., Fenn R.H., Physica C193, 90-98 (1992). Position-sensitive detectors in single-crystal diffractometry, McIntyre G.J., Neutron News 3, 15-19, (1992). Orientational ordering in liquid crystals : isotope labelling neutron diffraction experiments, Date R.W., Hamley I.W., Luckhurst G.R., Seddon J.M., Richardson R.M., Molecular Physics76, 951-977 (1992). Diene and arene compounds of zirconium and hafnium, Diamond G.M., Green M.L.H., Walker N.M., Howard J.A.K., Mason S.A., Journal of the Chemical Society Dalton Transactions 2641-2646 (1992). Entwicklung von Hochtemperaturneutronenstreuoefen und Strukturuntersuchungen an ZrSiO4 und ZrO2 bei Temperaturen bis 2300K, Mursic Z., Technisches Univsersitaet Muenchen, GER (1992). Disordered guest and water molecules. Three-center and flip-flop O-H...O hydrogen bonds in crystalline beta-cyclodextrin ethanol octahydrate at T = 295K: A neutron and X-ray diffraction study, Steiner T., Mason S.A., Saenger R W., Journal of the American Chemical Society113, 5676-5687 (1991). Neutron diffraction study of the hydrogen bonding in partially deuterated gamma-cyclodextrin,15.7D2O at T = 110 K, Ding J., Steiner T., Zabel V., Hingerty B.E., Mason S.A., Saenger W., Journal of the American Chemical Society 113, 8081-8089 (1991). Structure of superconducting tetragonal HoBa2Cu3O7-delta, Clamp M.E., Fenn R.H., Mills O.S., Mitchell P.W., Bramwell S.T., Physica B174, 364-366 (1991). Darstellung und Kristallstruktur von Na28In14Sn15, Blase W., Cordier G., Vogt T., Zeitschrift fuer Anorganische und Allgemeine Chemie606, 79-90 (1991). Direct location of the hydrido ligands in the dianion (H4Os10(CO)24)2- by a neutron diffraction study of its [(Ph3P)2N]+ salt at 20K, Bashall A.,Gade L.H.,Lewis J.,Johnson, B.F.G.,McIntyre G.J.,McPartlin M., Angewandte Chemie International Edition English30 1164-1167 (1991). Cooperative O-H...O hydrogen bonds in beta-cyclodextrin-ethanol-octahydrate at 15 K: A neutron diffraction study, Steiner T., Mason S.A., Saenger W., Journal of the American Chemical Society 112, 6184-6190 (1990). The determination of the location of ions and water around the DNA double helix, V.T. Forsyth, A. Mahendrasingam, E.D. Stevens, P.Langan, W. J. Pigram, S. A. Mason, W. Fuller, Proc. Ital. Phys. Soc. 25, 987-990 (1990). Neutron scattering from mixtures of isotopically labelled molecules. A new method for determining the orientational distribution function in liquid crystals, Richardson R.M., Allman J.M., McIntre G.J., Liquid Crystals 7, 701-719 (1990). X-ray and neutron high-angle fibre diffraction studies in the determination of hydration and ionic structure around DNA, V.T. Forsyth, A. Mahendrasingam, P. Langan, W.J. Pigram, E.D. Stevens, Y. Al-Hayalee, K. A. Bellamy, R.J. Greenall, S.A. Mason, W. Fuller, Inst. Phys. Conf. Ser. 101, 237 (1990). The first example of an intermolecular weak (agostic) gamma-methyl-metal interaction: the low temperature single crystal x-ray and neutron diffraction structure of (MgR2)infini(R=CH(SiMe3)2), Hitchcock P.B., Howard J.A.K., Lappert M.F., Leung W.P., Mason S.A., Chemical Communications 847-849 (1990). X-ray and neutron diffraction studies of PEEK, W. Fuller, C.R. Oates, A. Mahendrasingam, V.T. Forsyth, W.J. Pigram, R.J. Greenall, R.J. Oldman, M.J. Barry, D.J. Blundell, Inst. Phys. Conf. Ser. 101, 213 (1990). Molek?l- und Kristallstruktur der Phosphons?ure H3PO3-R?ntgen- und Neutronenbeugungsuntersuchungen an der Hydrogen- und der Deuterium-Verbindung, Becker G., Hausen H.D., Mundt O., Schwartz W., Wagner C.T., Vogt T., Zeitschrift fuer Anorganische und Allgemeine Chemie 591, 17-31 (1990). Neutron fibre diffraction studies of DNA hydration, V.T. Forsyth, A. Mahendrasingam, W.J. Pigram, R.J. Greenall, K. Bellamy, W. Fuller, S.A. Mason, Int. J. Biol. Macr. 11, 236 (1989). Neutron diffraction study of a one-layer monoclinic chlorite, Joswig W., Fuess H., Mason S.A., Clays and Clay Minerals 37, 511-514 (1989) The location of water around the DNA double helix, W. Fuller, V.T. Forsyth, A. Mahendrasingam, W.J. Pigram, R.J. Greenall, P. Langan, K. Bellamy, Y. Al-Hayalee, S.A. Mason, Physica B 156/157, 468 (1989). Binding of dimethyl sulfoxide to lysozyme in crystals, studied with neutron diffraction, Lehmann M.S., Stansfield R.F.D., Biochemistry 28, 7028-7033 (1989). On the low-temperature structural phase transitions in (CH3)4NCuCl3, Visser D., McIntyre G.J., Haije W.G., Maaskant W.J.A., Physica B156-157, 254-258 (1989). Diffraction studies of a T state haemoglobin, WALLER D.A., PhD Thesis, University of York, Department of Chemistry (1989). Detailed structure of an alpha cyclodextrin-cyclopentanone clathrate by neutron diffraction, LE BAS G., MASON S.A., RYSANEK N., TSOUCARIS G., International Symposium on Cyclodextrins, Proceedings of the Fourth International Conference on Cyclodextrins (eds HUBER O., SZEJTLI J.), 243-246 (World Scientific Press) (1988). Domain and crystal structure of superconducting Ba2YCu3O8-delta at 40 and 100 K by single-crystal neutron diffraction, MCINTYRE G.J., RENAULT A., COLLIN G., Physical Review B 37, 5148-5157 (1988). A general Lorentz correction for single-crystal diffractometers, MCINTYRE G.J., STANSFIELD R.F.D., Acta CrystallographicaA44, 257-262 (1988). Classical versus non-classical polyhydride complexes; single crystal neutron diffraction study of 2-Bis(diphenylphosphino)ethaneheptahydridorhenium(VII)[ReH7(dppe)]using a position-sensitive detector, HOWARD J.A.K., MASON S.A., JOHNSON O., DIAMOND I.C., CRENNELL S., KELLER P.A., SPENCER J.L., Chemical Communications 1502-1503 (1988). Neutron diffraction study of beta-cyclodextrin-ethanol-octahydrate, STEINER T., MASON S.A., SAENGER W., Zeitschrift fuer Kristallographie185, 166 (1988). Structure of Ba2YCu3O6.26 at 20 and 298K by single crystal neutron diffraction, RENAULT A., MCINTYREG.J., COLLIN G., POUGET J.P., COMES R., Journal de Physique 48, 1407-1412 (1987). Simulation de donnees en provenance d'experience de diffractometrie, BLANC J.Y., ILL internal report ILL86BL10T (1986). On-line evaluation of position-sensitive detector (PSD) diffraction data, STANSFIELD R.F.D., MCINTYREG.J. in Neutron scattering in the nineties, pp191-198 (International Atomic Energy Agency) (1985). Logiciel BRAGGVAX (en ligne) et BRAGGOFF (manuel) de reduction des donnees de D19, FILHOL A., GREENWOOD G., ILL internal report ILL84FI8T (1984). On line data reduction software for a 4-circle neutron diffractometer equipped with s fly's-eye area PSd, FILHOL A., THOMAS M., GREENWOOD G., BARTHELEMY A., in Position-sensitive detection of thermal neutrons (eds CONVERT P., FORSYTH J.B.), 351-357 (Academic Press, 1983). Test of the quality of data from DKDP using a 'Fly's-eye' neutron PSD, STANSFIELD R.F.D., THOMAS M., MASON S.A., NELMES R.J., TIBBALLS J.E., ZHONG W.L. in Position-sensitive detection of thermal neutrons (eds CONVERT P., FORSYTH J.B.), 365-371 (Academic Press, 1983). D19A and B: design and construction of a 4-circle neutron diffractometer with two-dimensional PSDs, THOMAS M., STANSFIELD R.F.D., BERNERON M., FILHOL A., GREE NWOOD G., in Position-sensitive detection of thermal neutrons (eds CONVERT P., FORSYTH J.B.), 344-350 (Academic Press, 1983). |